CORRELATION BETWEEN AGING TIME PERIOD OF METAL PRECURSOR SOL - PHASE COMPOSITION AND TEXTURAL PROPERTIES OF ZIRCONIA NANOPOWDERS

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creativework.keywordsmorphology, phase composition, phase transformation, sol-gel, zirconia nanoparticles
creativework.publisherUniversity of Chemical Technology and Metallurgyen
dc.contributor.authorMitkova E.
dc.contributor.authorStambolova I.
dc.contributor.authorStoyanova D.
dc.contributor.authorToteva V.
dc.contributor.authorDimitrov O.
dc.date.accessioned2024-07-10T14:27:06Z
dc.date.accessioned2024-07-10T14:51:06Z
dc.date.available2024-07-10T14:27:06Z
dc.date.available2024-07-10T14:51:06Z
dc.date.issued2024-01-01
dc.description.abstractThis article investigates the effect of the time of aging of ZrO2 powders, obtained from zirconium butoxide sols, stabilized using complexating agents on the volume phase fractions tetragonal phase (T) and baddeleyite crystalographic phase (B), pore size distribution and pore volume. It was proved that the aging time period influences ratio between these two polymorphs of zirconia. The sample Zr3d possesses the largest content of baddeleyite phase having the greatest crystallites in comparison to another two powders. The increasing of aging period leads to a gradual increase in (101) peak intensity of T phase, while all the samples are microporous regardless of the aging time. The longest time aged sample possesses higher pore volume and higher average pore diameter than the other two powders. The physico-chemical features of the prepared ZrO2 nanosized powders could be beneficial as catalysts/photocatalysts in different catalytic reactions, corrosion inhibition particles, etc.
dc.identifier.doi10.59957/jctm.v59.i1.2024.26
dc.identifier.issn1314-7978
dc.identifier.issn1314-7471
dc.identifier.scopusSCOPUS_ID:85183766316en
dc.identifier.urihttps://rlib.uctm.edu/handle/123456789/898
dc.language.isoen
dc.source.urihttps://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=85183766316&origin=inward
dc.titleCORRELATION BETWEEN AGING TIME PERIOD OF METAL PRECURSOR SOL - PHASE COMPOSITION AND TEXTURAL PROPERTIES OF ZIRCONIA NANOPOWDERS
dc.typeArticle
oaire.citation.issue1
oaire.citation.volume59
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